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<p class="MsoNormal"><span style="color:#1F497D;mso-fareast-language:EN-US">For what it is worth we used to run an SPTS Pegasus deep RIE etcher years ago, there is a Plasmatherm Versaline in its place now. I think we sold it ~6 years ago. We had many problems
with it towards the end of its life but o-ring seals were with regards to chamber or He leak rate were not one. We used the same set for possibly years at a time. I recall being advised on an official training course to boil them for a couple of hours in water
to remove the flatted edge before re-sealing the chamber which I never did, but always found to be quite interesting advice. I did have to rebuild the lower platen once due to a coolant leak and it did take me a about a day to get it to seal due to the complex
arrangement of o-rings. <o:p></o:p></span></p>
<p class="MsoNormal"><span style="color:#1F497D;mso-fareast-language:EN-US"><o:p> </o:p></span></p>
<p class="MsoNormal"><span style="color:#1F497D;mso-fareast-language:EN-US">If the black circle on the rear of the wafer is not the material breakdown of the o-ring itself, it could be micro-masking from rear wafer deposited polymer/spontaneous etching of Si
radicals giving a rough Si surface? Do not ask me why this would be the case but we find it is often the cause of unexpectedly blackened Si wafers removed from etch chambers.
<o:p></o:p></span></p>
<p class="MsoNormal"><span style="color:#1F497D;mso-fareast-language:EN-US"><o:p> </o:p></span></p>
<p class="MsoNormal"><span style="color:#1F497D;mso-fareast-language:EN-US">O.<o:p></o:p></span></p>
<p class="MsoNormal"><span style="color:#1F497D;mso-fareast-language:EN-US"><o:p> </o:p></span></p>
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<p class="MsoNormal"><b><span lang="EN-US">From:</span></b><span lang="EN-US"> labnetwork-bounces@mtl.mit.edu <labnetwork-bounces@mtl.mit.edu>
<b>On Behalf Of </b>Paolini, Steven<br>
<b>Sent:</b> 06 March 2019 22:32<br>
<b>To:</b> Mark Weiler <mweiler@andrew.cmu.edu>; Noah Clay <nclay@upenn.edu><br>
<b>Cc:</b> Fab Network <labnetwork@mtl.mit.edu><br>
<b>Subject:</b> Re: [labnetwork] STS DRIE Multiplex Lip Seal failures<o:p></o:p></span></p>
</div>
</div>
<p class="MsoNormal"><o:p> </o:p></p>
<p class="MsoNormal"><span lang="EN-US">My $0.02,<o:p></o:p></span></p>
<p class="MsoNormal"><span lang="EN-US">Black marks on the back of a wafer are not normal. I agree that there must have been a material change by the supplier perhaps to “value engineer” there consumables. What IS normal is O-rings growing a black crud on their
surfaces. This is simply O2 attacking organics regardless of the O-rings being out of the “ line of sight” of the plasma. A downstream etcher (two 90 degree gas shifts), will experience the same effect at a slower rate. We inspect them and if not cracked,
we clean them up until the wipes show minimum crud and put them back in for more service.<o:p></o:p></span></p>
<p class="MsoNormal"><span lang="EN-US">Oh yeah, I wholeheartedly agree with Julia that we should not forget that the LUR with backside He is the
<i>overall </i>LUR of the chamber and you could be mislead by some other fine leak not associated with the He seal.<o:p></o:p></span></p>
<p class="MsoNormal"><span lang="EN-US"><o:p> </o:p></span></p>
<div>
<p class="MsoNormal"><span lang="EN-US" style="font-size:14.0pt">Steve Paolini<o:p></o:p></span></p>
<p class="MsoNormal"><span lang="EN-US" style="font-size:14.0pt">Principal Equipment Engineer<o:p></o:p></span></p>
<p class="MsoNormal"><span lang="EN-US" style="font-size:14.0pt">Harvard University Center for Nanoscale Systems<o:p></o:p></span></p>
<p class="MsoNormal"><span lang="EN-US" style="font-size:14.0pt">11 Oxford St.<o:p></o:p></span></p>
<p class="MsoNormal"><span lang="EN-US" style="font-size:14.0pt">Cambridge, MA 02138<o:p></o:p></span></p>
<p class="MsoNormal"><span lang="EN-US" style="font-size:14.0pt">617- 496- 9816<o:p></o:p></span></p>
<p class="MsoNormal"><span lang="EN-US" style="font-size:14.0pt"><a href="mailto:spaolini@cns.fas.harvard.edu">spaolini@cns.fas.harvard.edu</a><o:p></o:p></span></p>
<p class="MsoNormal"><span lang="EN-US" style="font-size:14.0pt"><a href="http://www.cns.fas.harvard.edu">www.cns.fas.harvard.edu</a><o:p></o:p></span></p>
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<p class="MsoNormal"><span lang="EN-US"><o:p> </o:p></span></p>
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<p class="MsoNormal"><b><span lang="EN-US">From:</span></b><span lang="EN-US"> <a href="mailto:labnetwork-bounces@mtl.mit.edu">
labnetwork-bounces@mtl.mit.edu</a> <<a href="mailto:labnetwork-bounces@mtl.mit.edu">labnetwork-bounces@mtl.mit.edu</a>>
<b>On Behalf Of </b>Mark Weiler<br>
<b>Sent:</b> Wednesday, March 06, 2019 10:18 AM<br>
<b>To:</b> Noah Clay <<a href="mailto:nclay@upenn.edu">nclay@upenn.edu</a>><br>
<b>Cc:</b> Fab Network <<a href="mailto:labnetwork@mtl.mit.edu">labnetwork@mtl.mit.edu</a>><br>
<b>Subject:</b> Re: [labnetwork] STS DRIE Multiplex Lip Seal failures<o:p></o:p></span></p>
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<p class="MsoNormal"><span lang="EN-US"><o:p> </o:p></span></p>
<p class="MsoNormal"><span lang="EN-US">Hi Noah, <o:p></o:p></span></p>
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<p class="MsoNormal"><span lang="EN-US"><o:p> </o:p></span></p>
<div>
<p class="MsoNormal"><span lang="EN-US">We have the first version of the 100mm STS Multiplex DRIE whereby the wafer is mechanically clamped with weighted ceramic fingers, and the wafer is lifted with a tripod. Our LUR is 0.00 mTorr/min when new, but rises
to 15-20 mT/m within a week. We have an older HBC controller that indicates 6.5 for pressure at 2.33 flow rate... I apologize but don’t know the units for either. If these values are incorrect, it could be because they were adjusted to ensure a leak rate
would pass. I will need to go back over a decade in the logs to see if any changes were made over time...but, our rates and results have been consistent.<o:p></o:p></span></p>
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<p class="MsoNormal"><span lang="EN-US"><o:p> </o:p></span></p>
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<p class="MsoNormal"><span lang="EN-US">I believe the issue is material related, because we have our chamber lid o-ring and bottom ceramic o-ring failing with the same symptoms.<o:p></o:p></span></p>
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<p class="MsoNormal"><span lang="EN-US"><o:p> </o:p></span></p>
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<p class="MsoNormal"><span lang="EN-US">Thanks,<o:p></o:p></span></p>
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<div>
<p class="MsoNormal"><span lang="EN-US"><o:p> </o:p></span></p>
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<p class="MsoNormal"><span lang="EN-US">Mark<o:p></o:p></span></p>
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<p class="MsoNormal"><span lang="EN-US"><o:p> </o:p></span></p>
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<p class="MsoNormal" style="margin-bottom:12.0pt"><span lang="EN-US"><o:p> </o:p></span></p>
<div id="AppleMailSignature">
<p class="MsoNormal"><b><span lang="EN-US">Mark Weiler</span></b><span lang="EN-US"><br>
Equipment & Facilities Manager <o:p></o:p></span></p>
<div>
<p class="MsoNormal"><span lang="EN-US">Claire and John Bertucci Nanotechnology Laboratory<br>
Electrical and Computer Engineering | Carnegie Mellon University<br>
<a href="x-apple-data-detectors://3/1">5000 Forbes Ave., Pittsburgh, PA 15213-3890</a><br>
T: <a href="tel:412.268.5430">412.268.2471</a><br>
F: <a href="tel:412.268.3497">412.268.3497</a><br>
<a href="https://emea01.safelinks.protection.outlook.com/?url=https%3A%2F%2Furldefense.proofpoint.com%2Fv2%2Furl%3Fu%3Dhttp-3A__www.ece.cmu.edu_%26d%3DDwMGaQ%26c%3DWO-RGvefibhHBZq3fL85hQ%26r%3D-H4Z_jeDfTYjnKPXor15vLwzBllmg8gFrb9m_k9OGks%26m%3Dt7HorgNjXk4V-6m_P8F1UoRXoyMkEleQx7WVKYxreVA%26s%3Di62eu2c6bno0Xe4sH3YpYnU2wd_7O1xBtpg2DbBFxDg%26e%3D&data=01%7C01%7Codc1n08%40soton.ac.uk%7Cc7141276cb754a286d2c08d6a296cb03%7C4a5378f929f44d3ebe89669d03ada9d8%7C1&sdata=5mdpJZLpE5%2BS%2F6EZ%2FBcN1Udy7by%2FKlPc0nbyYnnOzwE%3D&reserved=0">www.ece.cmu.edu</a><br>
<a href="https://emea01.safelinks.protection.outlook.com/?url=https%3A%2F%2Furldefense.proofpoint.com%2Fv2%2Furl%3Fu%3Dhttp-3A__nanofab.ece.cmu.edu_%26d%3DDwMGaQ%26c%3DWO-RGvefibhHBZq3fL85hQ%26r%3D-H4Z_jeDfTYjnKPXor15vLwzBllmg8gFrb9m_k9OGks%26m%3Dt7HorgNjXk4V-6m_P8F1UoRXoyMkEleQx7WVKYxreVA%26s%3DltoSF70VzK-YU-BI1rqnTp6iKgKIYVF_gDu1-r_Lk4E%26e%3D&data=01%7C01%7Codc1n08%40soton.ac.uk%7Cc7141276cb754a286d2c08d6a296cb03%7C4a5378f929f44d3ebe89669d03ada9d8%7C1&sdata=10jWfI8F0GpPkfM%2BJvBVEi%2FIN0etCOzPTFgCsb1CUpw%3D&reserved=0">nanofab.ece.cmu.edu</a><o:p></o:p></span></p>
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<div>
<p class="MsoNormal" style="margin-bottom:12.0pt"><span lang="EN-US"><br>
On Mar 6, 2019, at 09:19, Noah Clay <<a href="mailto:nclay@upenn.edu">nclay@upenn.edu</a>> wrote:<o:p></o:p></span></p>
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<blockquote style="margin-top:5.0pt;margin-bottom:5.0pt">
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<p class="MsoNormal"><span lang="EN-US">Mark, <o:p></o:p></span></p>
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<p class="MsoNormal"><span lang="EN-US"><o:p> </o:p></span></p>
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<p class="MsoNormal"><span lang="EN-US">I have seen blackening on the back of the wafer when clamping is poor. Most recently, this was due the e-chuck having been etched excessively and/or polymer redep on the chuck from the endpoint clean step (cleans used
to be run without a wafer; we now use SiC). <o:p></o:p></span></p>
</div>
<div>
<p class="MsoNormal"><span lang="EN-US"><o:p> </o:p></span></p>
</div>
<div>
<p class="MsoNormal"><span lang="EN-US">What are your backside He leak rate set points and actual values? We run our etch process at -5C...(SPTS Rapier platform).<o:p></o:p></span></p>
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<div>
<p class="MsoNormal"><span lang="EN-US"><o:p> </o:p></span></p>
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<p class="MsoNormal"><span lang="EN-US">Thanks,<o:p></o:p></span></p>
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<div>
<p class="MsoNormal" style="margin-bottom:12.0pt"><span lang="EN-US">Noah<o:p></o:p></span></p>
<div id="AppleMailSignature">
<p class="MsoNormal"><span lang="EN-US">Sent from my iPhone<o:p></o:p></span></p>
</div>
<div>
<p class="MsoNormal" style="margin-bottom:12.0pt"><span lang="EN-US"><br>
On Mar 5, 2019, at 15:44, Mark Weiler <<a href="mailto:mweiler@andrew.cmu.edu">mweiler@andrew.cmu.edu</a>> wrote:<o:p></o:p></span></p>
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<p class="MsoNormal"><span lang="EN-US">Hello Everyone, <o:p></o:p></span></p>
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<p class="MsoNormal"><span lang="EN-US"><o:p> </o:p></span></p>
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<p class="MsoNormal"><span lang="EN-US">We have gone through seven new lip seals purchased form Orbotech/SPTS. They are often failing before we even finish qualifying the system, or within a month thereafter.
<o:p></o:p></span></p>
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<p class="MsoNormal"><span lang="EN-US"><o:p> </o:p></span></p>
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<p class="MsoNormal"><span lang="EN-US">Our our process is stable with power and parameters not deviating over the past decade. However, I ordered the most recent batch of lip seals because the wafer seals we had been using were coming out with black residue
after only a few runs… however, the current ones do the same. Not only have the lips seals disintegrated, but the chamber lid o-ring and bottom ceramic spool o-ring have also failed with black rubber material shedding off. It’s as if they are made of Buna
and not meant for this application.<o:p></o:p></span></p>
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<div>
<p class="MsoNormal"><span lang="EN-US"><o:p> </o:p></span></p>
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<div>
<p class="MsoNormal"><span lang="EN-US">Our process is typical Bosch with 100 sccm C4F8 and 20 sccm O2 for etching switching off with ~50 Sccm SF6 for passivation at a processing pressure of 15 mTorr, Coil power 600-800W, Platen power 100-150W, Bias voltage
50-100v (up to 200 peak-to-peak), Platen temp at 19 degrees, Lid temp 41 degrees. Qual wafers are new bare Silicon. Etch rates are normal and stable with 10+ years of data…. we just can’t complete the work due to failing seals.<o:p></o:p></span></p>
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<p class="MsoNormal"><span lang="EN-US"><o:p> </o:p></span></p>
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<p class="MsoNormal"><span lang="EN-US">Our chamber base pressure is between 1E-8 and 5E-8 Torr each morning. When we put in a brand new seal and run only the LUR, it passes with 0.00 mTorr/minute leak rate. That jumps to 3.00 mTorr/m after only 30 minutes
of the SPTS recommended O2 Clean… then rises as time and more runs progress. Wafers are coming out with black rings on their backsides. <o:p></o:p></span></p>
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<p class="MsoNormal"><span lang="EN-US"><o:p> </o:p></span></p>
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<p class="MsoNormal"><span lang="EN-US">This should not be happening, and I believe it is due to incorrect material of the lip seals and o-rings. I am pinging the network, though, to see if there might be a parameter change we need to effect that may assist
us.<o:p></o:p></span></p>
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<p class="MsoNormal"><span lang="EN-US"><o:p> </o:p></span></p>
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<p class="MsoNormal"><span lang="EN-US">Have any of you seen this before?<o:p></o:p></span></p>
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<p class="MsoNormal"><span lang="EN-US"><o:p> </o:p></span></p>
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<p class="MsoNormal"><span lang="EN-US">Best regards,<o:p></o:p></span></p>
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<p class="MsoNormal"><span lang="EN-US"><o:p> </o:p></span></p>
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<p class="MsoNormal"><span lang="EN-US">Mark<o:p></o:p></span></p>
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<p class="MsoNormal" style="margin-bottom:12.0pt"><span lang="EN-US" style="font-size:9.0pt;font-family:"Helvetica",sans-serif;color:black"><o:p> </o:p></span></p>
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<p class="MsoNormal"><span lang="EN-US" style="font-size:9.0pt;font-family:"Helvetica",sans-serif;color:black">________________________________________________________________<o:p></o:p></span></p>
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<p class="MsoNormal"><span lang="EN-US" style="font-size:9.0pt;font-family:"Helvetica",sans-serif;color:black"><o:p> </o:p></span></p>
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<p class="MsoNormal"><span lang="EN-US" style="font-size:9.0pt;font-family:"Helvetica",sans-serif;color:black">Mark Weiler<o:p></o:p></span></p>
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<p class="MsoNormal"><span lang="EN-US" style="font-size:9.0pt;font-family:"Helvetica",sans-serif;color:black">Equipment & Facilites Manager<o:p></o:p></span></p>
</div>
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<p class="MsoNormal"><span lang="EN-US" style="font-size:9.0pt;font-family:"Helvetica",sans-serif;color:black">Clair and John Bertucci Nanotechnology Laboratory<o:p></o:p></span></p>
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<div>
<p class="MsoNormal"><span lang="EN-US" style="font-size:9.0pt;font-family:"Helvetica",sans-serif;color:black">Eden Hall Nanofabrication Cleanroom<o:p></o:p></span></p>
</div>
<div>
<p class="MsoNormal"><span lang="EN-US" style="font-size:9.0pt;font-family:"Helvetica",sans-serif;color:black">Carnegie Mellon University<o:p></o:p></span></p>
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<p class="MsoNormal"><span lang="EN-US" style="font-size:9.0pt;font-family:"Helvetica",sans-serif;color:black">P: 412-268-2471<o:p></o:p></span></p>
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<p class="MsoNormal"><span lang="EN-US" style="font-size:9.0pt;font-family:"Helvetica",sans-serif;color:black"><o:p> </o:p></span></p>
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</span><span lang="EN-US"><a href="https://emea01.safelinks.protection.outlook.com/?url=https%3A%2F%2Furldefense.proofpoint.com%2Fv2%2Furl%3Fu%3Dhttps-3A__www.linkedin.com_in_marksbasics%26d%3DDwMGaQ%26c%3DWO-RGvefibhHBZq3fL85hQ%26r%3D-H4Z_jeDfTYjnKPXor15vLwzBllmg8gFrb9m_k9OGks%26m%3Dt7HorgNjXk4V-6m_P8F1UoRXoyMkEleQx7WVKYxreVA%26s%3DyI38qZlDy_Ubr2PUVtwfgDDQRJKod8Tta6_CMCMvW9M%26e%3D&data=01%7C01%7Codc1n08%40soton.ac.uk%7Cc7141276cb754a286d2c08d6a296cb03%7C4a5378f929f44d3ebe89669d03ada9d8%7C1&sdata=QvVGUI%2BpVnipmZe5NCAeKL338LZJmzCCjru1d%2FveYKY%3D&reserved=0"><span style="font-size:9.0pt;font-family:"Helvetica",sans-serif"><images.png>
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<p class="MsoNormal"><span lang="EN-US">_______________________________________________<br>
labnetwork mailing list<br>
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<a href="https://emea01.safelinks.protection.outlook.com/?url=https%3A%2F%2Furldefense.proofpoint.com%2Fv2%2Furl%3Fu%3Dhttps-3A__mtl.mit.edu_mailman_listinfo.cgi_labnetwork%26d%3DDwMGaQ%26c%3DWO-RGvefibhHBZq3fL85hQ%26r%3D-H4Z_jeDfTYjnKPXor15vLwzBllmg8gFrb9m_k9OGks%26m%3Dt7HorgNjXk4V-6m_P8F1UoRXoyMkEleQx7WVKYxreVA%26s%3DzuEJRDi_Al5AddBo2kikVmK-6sbtts2_rWSy8-A5ejs%26e%3D&data=01%7C01%7Codc1n08%40soton.ac.uk%7Cc7141276cb754a286d2c08d6a296cb03%7C4a5378f929f44d3ebe89669d03ada9d8%7C1&sdata=6Pt5bNH4sEmE%2BlCMYAimiPwWjMnScGa65jsWgs9zNj8%3D&reserved=0">https://mtl.mit.edu/mailman/listinfo.cgi/labnetwork</a><o:p></o:p></span></p>
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